Dinucleotides as simple models of the base stacking-unstacking component of DNA 'breathing' mechanisms

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Date

2021-01

Authors

Beyerle, Eric R.
Dinpajooh, Mohammadhasan
Ji, Huiying
von Hippel, Peter H.
Marcus, Andrew H.
Guenza, Marina G.

Journal Title

Journal ISSN

Volume Title

Publisher

Oxford Academic

Abstract

Regulatory protein access to the DNA duplex 'interior' depends on local DNA 'breathing' fluctuations, and the most fundamental of these are thermally-driven base stacking-unstacking interactions. The smallest DNA unit that can undergo such transitions is the dinucleotide, whose structural and dynamic properties are dominated by stacking, while the ion condensation, cooperative stacking and inter-base hydrogen-bonding present in duplex DNA are not involved. We use dApdA to study stacking-unstacking at the dinucleotide level because the fluctuations observed are likely to resemble those of larger DNA molecules, but in the absence of constraints introduced by cooperativity are likely to be more pronounced, and thus more accessible to measurement. We study these fluctuations with a combination of Molecular Dynamics simulations on the microsecond timescale and Markov State Model analyses, and validate our results by calculations of circular dichroism (CD) spectra, with results that agree well with the experimental spectra. Our analyses show that the CD spectrum of dApdA is defined by two distinct chiral conformations that correspond, respectively, to a Watson-Crick form and a hybrid form with one base in a Hoogsteen configuration. We find also that ionic structure and water orientation around dApdA play important roles in controlling its breathing fluctuations.

Description

14 pages

Keywords

Circular Dichroism, DNA, Markov Chains, Molecular Models, Sodium Chloride

Citation

Beyerle ER, Dinpajooh M, Ji H, von Hippel PH, Marcus AH, Guenza MG. Dinucleotides as simple models of the base stacking-unstacking component of DNA 'breathing' mechanisms. Nucleic Acids Res. 2021 Feb 26;49(4):1872-1885. doi: 10.1093/nar/gkab015. PMID: 33503257; PMCID: PMC7913701.